X-ray diffraction facility at the XAS LABOur group has recently installed a four-circle compact diffractometer in the framework of a collaboration with the University of Brescia (Prof. L. E. Depero, INSTM and Laboratorio di Strutturistica Chimica).
The diffractometer is a KM4 KUMA using a Four-circle kappa goniometer with a point detector (NaI scintillator). The more recent version of this instrument is the Xcalibur diffractometer (Oxford Diffraction ). Our setup features:
We are now refining the alignment and performances of the diffractometer and we shall be shortly able to perform classic single-crystal structural refinements relevant to protein and macromolecular crystallography, minerals, and compounds of interest for chemistry and physics. The project of our group is focussed in installing a high-pressure DAC cell for crystallographic measurements under extreme conditions. |
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